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Begin
with 6g colloidal Degussa P25 TiO2
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Incrementaly add
1mL nitric or acetic acid solution (pH 3-4) nine
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times, while
grinding in mortar and pestle
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Add the 1mL
addition of dilute acid solution only after previous
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mixing creates a
uniform, lump-free paste
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Process takes
about 30min and should be done in ventilated hood
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Let equilibrate
at room temperature for 15 minutes
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